Elemental Analysis
Elemental
Analysis belongs to one of our earliest and most often requested services.
It serves two purposes:
- To provide for pure materials elemental composition
for which an empirical formula can be derived.
- To assess the purity of pharmaceutical preparations, chemicals, and
high quality solvents.
Our Organic Elemental Microanalysis uses micro chemical techniques to
determine weight-% of elements accurately to 0.3% with milligram amounts
of an organic substance.
CH/CHN/O 
Our
experienced staff uses the Perkin Elmer 2400 CHN analyzer to provide accurate
and fast results.
Most
samples are analyzed on the day they are received.
Sample
requirement: 3.0 mg (often 1.0 mg is sufficient).
Reporting
limits: from detection limit of 0.02% to range of 100%.
S-F-Cl-Br-I-P
Generally
Titration, Ion Chromatography and specific element methods are used for
best micro analytical results.
To
obtain optimized analytical methods for best accuracy, various analytical
techniques are used to address a large variety of cross-interferences
and concentration levels.
Sample
requirement: 5-10 mg/element (assuming that 5 % of the element is present).
Reporting
limits: from detection limit of 0.02% to range of 100%, depending on the
method used.
KF
We use the
coulometric water determination according to the Karl Fisher method (KF-H2O).
The detection limit is 10 mg to high % levels.
Sample
requirement: 3-10 mg.
Reporting
limits: from range of 0.1 % to high percent level.
Ash
Ash can be
defined as non-combustible inorganic residue, Residue on Ignition (ROI).
Sulfated
ash can also be determined.
Sample
requirement: 10 mg.
Reporting limits: as
low as 0.1 % ash reported.
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